NF EN ISO 4259-1

NF EN ISO 4259-1

December 2017
Standard Current

Petroleum and related products - Precision of measurement methods and results - Part 1 : determination of precision data in relation to methods of test

ISO 4259-1:2017 specifies the methodology for the design of an Interlaboratory Study (ILS) and calculation of precision estimates of a test method specified by the study. In particular, it defines the relevant statistical terms (Clause 3), the procedures to be adopted in the planning of ILS to determine the precision of a test method (Clause 4), and the method of calculating the precision from the results of such a study (Clauses 5 and 6). The procedures in ISO 4259-1:2017 have been designed specifically for petroleum and petroleum related products, which are normally considered as homogeneous. However, the procedures described in ISO 4259-1:2017 can also be applied to other types of homogeneous products. Careful investigations are necessary before applying ISO 4259-1:2017 to products for which the assumption of homogeneity can be questioned.

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Main informations

Collections

National standards and national normative documents

Publication date

December 2017

Number of pages

85 p.

Reference

NF EN ISO 4259-1

ICS Codes

75.080   Petroleum products in general

Classification index

M07-033-1

Print number

1

International kinship

European kinship

EN ISO 4259-1:2017
Sumary
Petroleum and related products - Precision of measurement methods and results - Part 1 : determination of precision data in relation to methods of test

ISO 4259-1:2017 specifies the methodology for the design of an Interlaboratory Study (ILS) and calculation of precision estimates of a test method specified by the study. In particular, it defines the relevant statistical terms (Clause 3), the procedures to be adopted in the planning of ILS to determine the precision of a test method (Clause 4), and the method of calculating the precision from the results of such a study (Clauses 5 and 6).

The procedures in ISO 4259-1:2017 have been designed specifically for petroleum and petroleum related products, which are normally considered as homogeneous. However, the procedures described in ISO 4259-1:2017 can also be applied to other types of homogeneous products. Careful investigations are necessary before applying ISO 4259-1:2017 to products for which the assumption of homogeneity can be questioned.

Replaced standards (1)
NF EN ISO 4259
November 2006
Standard Cancelled
Petroleum products - Determination and application of precision data in relation to methods of test

<p>ISO 4259:2006 covers the calculation of precision estimates and their application to specifications. In particular, it contains definitions of relevant statistical terms, the procedures to<b> </b>be adopted in the planning of an inter-laboratory test programme to determine the precision of a test method, the method of calculating the precision from the results of such a programme, and the procedure to be followed in the interpretation of laboratory results in relation both to precision of the test methods and to the limits laid down in specifications.</p> <p>The procedures in ISO 4259:2006 have been designed specifically for petroleum and petroleum-related products, which are normally homogeneous. However, the procedures described in this International Standard can also be applied to other types of homogeneous products. Careful investigations are necessary before applying ISO 4259:2006 to products for which the assumption of homogeneity can be questioned.</p>

Table of contents
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  • 1 Domaine d'application
  • 2 Références normatives
  • 3 Termes et définitions
  • 4 Étapes de l'organisation d'un essai interlaboratoires pour la détermination de la fidélité d'une méthode d'essai
  • 5 Traitement statistique des résultats de l'ILS
  • 6 Analyse de la variance, calcul et expression des estimations de fidélité
  • 7 Ratio R/r
  • Annexe A Détermination du nombre d'échantillons requis
  • Annexe B Établissement de la formule d'estimation du nombre de laboratoires et d'échantillons requis pour atteindre les 30 degrés de liberté minimum
  • Annexe C Notation et essais
  • Annexe D Représentation des procédures utilisant les résultats de l'ILS pour l'indice de brome et les tableaux statistiques de brome
  • Annexe E Types de dépendance et transformations correspondantes
  • Annexe F Analyse de régression linéaire pondérée
  • Annexe G Règles d'arrondissage des résultats
  • Annexe H Technique GESD pour identifier simultanément plusieurs valeurs aberrantes d'un jeu de donnée
  • Annexe I Glossaire
  • Bibliographie
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